35
B FIRST SECTION OF THE VOYAGE
1 Chemistry (G, Weichart)
Chemical parameters also served the purpose of
characterization of the different watermasses, apart
from temperature and salinity (see Contribution No,
384 du Departement Scientifique, Centre Oc&anologique
de Bretagne), During the cycle sections 2 and 6, the
chemistry working team of the Deutsches Hydrographi-
sches Institut determined the dissolved silicate,
the dissolved inorganic phosphate, and the dissolved
oXygen,
The water samples were taken by a Bissett-Berman probe,
Twelve water samplers were attached to this probe, and
they could be closed - at the water depths desired —-
by remote control from on board ship.
The determination of the dissolved si 1 i-
ca te was carried out with a Technicon Company
Auto-Analyzer II, according to the silicomolybdenum
blue method, as recommended in the firm's analysis
instructions,
Ammonium molybdate solution: 1 % ammonium
in 0.1 N sulphuric acid,
Flow rate: 0.51 ml/min,
Oxalic acid solution: 5 % oralic acid in distilled
water.
Flow rate: 0,38 ml/min,
Ascorbic acid solution: 1,76 % ascorbic acid
distilled water.
Flow rate: 0,39 ml/min.
Flow rate of the seawater to be inve.tigated;
0.38 ml/min,
Time of passage of the seawater through the whole
system (from the sample taker to the cuvette):
ca, 8 min,
No. of samples per hour: 10,
Calibration substance: sodiumfluv---
vybdate
ıte (Na„SiFc).