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Oil Spill identification - Round Robin 20045
2.11 Swedish National Laboratory of Forensic Science
(SKL)
Contact: M. Kallberg
SKL is the only forensic laboratory in Sweden and thus all kinds of
investigations are performed, mainly to assist the police. The total
number of persons employed is about 240. SKL has four departments:
biology+morphology
documents+IT
drugs
chemistry+technique+weapon.
One group of nine persons is dealing with investigations related to fire,
oil and environment. A big part of this is the analyses of oil samples in
cases of fire-raising (e.g. gasoline and kerosene) and environmental
contaminations.
SKL does not (yet) have a home page on the Internet in English, they
only have information in Swedish: http://www.skl.polisen.se/.
The samples were analysed according to the standard procedure for oil
investigation at the Swedish National Laboratory of Forensic Science.
The method used is based on the "Nordtest method NT CHEM 001
Edition 2" which may be found also in the Internet:
http://www.nordicinnovation.net/nordtestfiler/chem001 .pdf
The oil samples were diluted with dichloromethane and analysed with
gas chromatography with flame ionisation detection.
If there are differences between the samples that cannot be explained
by weathering effects we conclude that the samples are not identical
(have not been identical at the moment of discharge) and make no
further investigations.
If the results can be explained by weathering effects we continue by
running the extracts on GC-MS in SIM mode
=> According to the result of our analysis there is a positive match between
spill samples (Extract I and II) and Source I. Between the spilled samples
(Extract I and II) and the Source II there is a non-match. We express this in
the same way as with other forensic comparisons, please see the last page of
the SKL report.
The findings show with certainty that the oil spill sample Extract I was
identical with the bilge oil sample Source I at the time of discharge (Level
+4).
The findings strongly indicate that the oil spill sample Extract II was
identical with the bilge oil sample Source I at the time of discharge (Level
+3).
The findings show with certainty that none of the oil spill samples
Extract I or II were identical with the bilge oil sample Source II (Level -
4).